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A new family of heterometal–organic frameworks has been prepared by two synthesis strategies, in which IFMC‐26 and IFMC‐27 are constructed by self‐assembly and IFMC‐28 is obtained by stepwise synthesis based on the metalloligand (IFMC=Institute of Functional Material Chemistry). IFMC‐26 is a (3,6)‐connected net and IFMC‐27 is a (4,8)‐connected 3D framework. The metalloligands {Ni(H4L)}(NO3)2 are connected...
Three mesoporous metal‐organic frameworks (MOFs) with rare corundum‐type topology and size‐tailored cages are constructed by length‐extendable tetratopic ligands. All the MOFs show selective CO2 uptake over N2 and their CO2 uptake capabilities are discriminated with different cage sizes. The MOFs can serve as hosts for encapsulating extra‐framework lanthanide cations, and be applicable in column‐chromatographic...
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