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Chemical treatment of transition‐metal dichalcogenides (TMDs) by organic superacid bis(trifluoromethane) sulfonamide TFSI, has been proved as an effective route to reduce the density of sulfur vacancies and improve photoluminescence quantum yield (PL QY) of monolayer TMDs (1L‐TMDs). However, such kind of functional organic superacid is only limited to the TFSI so far, and the underlying mechanism...
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