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In this paper, Li2(BH4)(NH2) and Li4(BH4)(NH2)3 compounds were prepared through different synthesis approaches (ball milling, annealing treatment and liquid quenching) and characterized by X-ray diffraction and solid-state NMR. The thermal analysis of samples with various (LiBH4)1−x(LiNH2)x compositions (0 ≤ x ≤ 1) have been performed by High Pressure DSC. Lattice constants, chemical shifts and relative...
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