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The potent oxidizer and highly shock‐sensitive binary noble‐gas oxide XeO3 interacts with CH3CN and CH3CH2CN to form O3XeNCCH3, O3Xe(NCCH3)2, O3XeNCCH2CH3, and O3Xe(NCCH2CH3)2. Their low‐temperature single‐crystal X‐ray structures show that the xenon atoms are consistently coordinated to three donor atoms, which results in pseudo‐octahedral environments around the xenon atoms. The adduct series provides...
Acetonitrile and the potent oxidative fluorinating agent XeF6 react at −40 °C in Freon‐114 to form the highly energetic, shock‐sensitive compounds F6XeNCCH3 (1) and F6Xe(NCCH3)2⋅CH3CN (2⋅CH3CN). Their low‐temperature single‐crystal X‐ray structures show that the adducted XeF6 molecules of these compounds are the most isolated XeF6 moieties thus far encountered in the solid state and also provide the...
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