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Treatment of a solid mixture of KBH 4 with six equivalents of 3,5-diisopropylpyrazole (iPr 2 pzH) at 180°C afforded KTp iPr2 (iPr 2 PzH) 3 in 53% yield. KBp iPr2 was synthesized in 56% yield by treatment of a 1:2M ratio of KBH 4 and iPr 2 PzH in refluxing dimethylacetamide. Treatment of MI 2 (M=Ca, Sr, Ba) with two equivalents...
Treatment of [(2,6-iPr2C6H3)NC(tBu)CH2C(tBu)N(2,6-iPr2C6H3)](LAr′H) with potassium hydride in tetrahydrofuran afforded K(η1-LAr′)(THF)3 (89%) as a yellow crystalline solid after workup. The crystal structure of K(η1-LAr′)(THF)3 revealed an open monomeric molecule in which the potassium ion is bonded to three tetrahydrofuran ligands and one η 1 -β-diketiminato ligand through one of the nitrogen...
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