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A ligand makes a difference: The reactivity of a dimolybdenum phosphinidene complex with alkenes and alkynes is substantially modified by the presence of two‐electron donors such as CO or CNXyl (Xyl=xylyl). Under these multicomponent reaction conditions, rapid formation of phosphametallacyclopentene rings takes place at room temperature. These reactions proceed in all cases with very high chemo‐ and...
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