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The gallium(I)tris(trimethylsilyl)silyl compound {GaSi(SiMe 3 ) 3 } 4 (1) is obtained by reaction of Ga 2 Cl 4 -2dioxane with LiSi(SiMe 3 ) 3 -3THF. The crystal structure of 1 reveals a tetramer with a nearly regular tetrahedral framework of gallium atoms. The gallium-gallium distances average 258.4 pm. Ab initio calculations on various substituted...
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