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Cold‐Spray Ionization mass spectrometry (CSI‐MS) that can be compared to an electrospray ionization (ESI) source acting with a nebulizing gas cooled by liquid nitrogen is used for analyzing reline as Deep Eutectic Solvent (DES). The association of cholinium chloride salts with urea molecules is evidenced in negative CSI‐MS through the chloride adduct formation. The structure of the supramolecular...
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