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An enhancement in the electron‐transfer rates of metal complexes confined to a nanoscale environment within a sodium bis(2‐ethylhexyl)sulfosuccinate/water/isooctane reverse micelle (RM) are reported. The rate constants increase up to two orders of magnitude relative to those in bulk water. These rate enhancements are attributed to changes in solvation (owing to location within the RM) and ion pairing.
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