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Two aspects of Group 13 metal chemistry are surveyed in the light of recent matrix-isolation and quantum chemical studies. The first concerns derivatives of the metals Al, Ga and In (M) in formal oxidation states less than +3: these include the M 0 derivatives ML n , where L=CO, N 2 , NH 3 or PH 3 , and n=1 or 2; the M I derivatives MX, where X=H, CH...
The mixed gallium-boron hydride HGa(BH 4 ) 2 has been synthesized by the reaction between lithium tetrahydroborate and gallium(III) chloride or dichlorogallane, [HGaCl 2 ] 2 , in the absence of a solvent at 238-263 K. The compound, which decomposes to elemental gallium, dihydrogen and B 2 H 6 at ambient temperatures, has been characterized by chemical...
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