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The metathetical reactions between SnBr4 and Li2[E'C(PPh2E)2] in toluene produce the homoleptic tin(IV) complexes Sn[E′C(PPh2E)2]2 [E = E′ = S (1b); E = S, E′ = Se (1c)], which were isolated as red crystals and structurally characterized by X‐ray crystallography. The metrical parameters of these octahedral complexes are compared with those of the all‐selenium analog Sn[E′C(PPh2E)2]2 (E = E′ = Se,...
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