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Experimental and simulated 14 N MAS NMR spectra of the NH4+ ions in the two polymorphs, mS60 and mP60, of (NH 4 ) 2 MoO 4 are used to illustrate that a long-term stability of rotor-controlled MAS frequencies to 0.1Hz can be achieved using commercial instrumentation (MAS speed controller and 7.5mm MAS probe with a single marked rotor) attached to a highly pressure-stabilized...
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