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Utilizing a standard spin Hamiltonian for an S=32 spin system, we fit complete X-band powder EPR spectra of the Cr(oxalate)33- anion diluted into K 3 [Co(oxalate) 3 ]·3H 2 O. By using models for the bandshape and bandwidths of varying degree of flexibility, we show that the successful outcome of such a fitting endeavour very much depends on the used bandshape–bandwidth model...
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