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The crystallization behavior of polychloroprene rubber (CR) has been studied in this work. Differential scanning calorimetry (DSC) was applied to characterize the crystallization behavior. And X‐ray diffraction was applied to determine the impact of crosslinking on the crystallization of CR. Synchrotron X‐ray diffraction (SXRD) method was applied to study the dynamic crystalline behavior. On the basis...
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