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This works introduces hypervalent bis‐catecholato silicon compounds as versatile sources of alkyl radicals upon visible‐light photocatalysis. Using Ir[(dF(CF3)ppy)2(bpy)](PF6) (dF(CF3)ppy=2‐(2,4‐difluorophenyl)‐5‐trifluoromethylpyridine, bpy=bipyridine) as catalytic photooxidant, a series of alkyl radicals, including highly reactive primary ones can be generated and engaged in various intermolecular...
Hypervalente Verbindungen. Über die photokatalytische Oxidation von Silicaten zu Alkylradikalen für homolytische Transformationen wird von L. Fensterbank et al. in der Zuschrift auf S. 11576 ff. berichtet.
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