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An efficient semisynthesis of silylated l‐amino acids by reaction of silylated benzaldehydes with a phosphonium l‐amino acid used as a Wittig reagent is described. The efficiency of the silylated l‐amino acids in peptide synthesis was investigated by coupling both the carboxylic acid and the amino moiety with l‐alanine and phenylalanine derivatives, respectively. The silylated derivatives were treated...
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