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A facile solvothermal approach was used to prepare brookite-type TiO2 nanocrystals with different phase content and structure, accomplished by adjusting the ratio of TiCl4 to t-BuOH. The obtained biphasic brookite/rutile TiO2 nanocrystals showed a high brookite weight content (72%). The photocatalytic degradation of phenol under UV-irradiation was used to determine the synergetic effect from the combination...
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