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A facile one‐step strategy is explored to achieve uniform luminescent Au nanoparticles (AuNPs) in a two‐dimensional ultrathin silica matrix based on simultaneous reaction and assembly at the liquid–liquid interface. The as‐prepared AuNPs/silica nanocomposites can be further employed to fabricate micrometer‐thick films with bifunctional luminescent and superhydrophobic properties. Such a versatile...
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