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A one-pot synthesis of rose-like Pd–Fe3O4 nanocomposites via the controlled thermal decomposition of Fe(CO)5 and reduction of Pd(OAc)2 is reported. This rose-like Pd–Fe3O4 composite structure has a high surface area owing to the individual Pd–Fe3O4 nanosheets, which imparted a high catalytic activity for Sonogashira coupling reactions. Moreover, the catalyst also demonstrated magnetic recyclability.
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