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We show that triple-quantum–single-quantum (TQ–SQ) correlation spectra of crystalline and disordered solids can be obtained under MAS using pulse sequences based on through-bond J-couplings. The feasibility of the experiments in coupled spin-1/2 systems is demonstrated for fully 13 C-labelled l-alanine and Pb 3 P 4 O 13 crystalline compounds, considered as model three-spin...
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