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MFM‐300(Al) shows reversible uptake of NH3 (15.7 mmol g−1 at 273 K and 1.0 bar) over 50 cycles with an exceptional packing density of 0.62 g cm−3 at 293 K. In situ neutron powder diffraction and synchrotron FTIR micro‐spectroscopy on ND3@MFM‐300(Al) confirms reversible H/D site exchange between the adsorbent and adsorbate, representing a new type of adsorption interaction.
Das poröse MFM‐300(Al) kann Ammoniakgas bei Raumtemperatur in über 50 Adsorptions‐ und Freigabezyklen ohne Zersetzung speichern und freisetzen. Wie S. Yang, M. Schröder et al. in ihrer Zuschrift auf S. 14994 berichten, wird eine hohe Packungsdichte von Ammoniak beobachtet. In‐situ‐Neutronenpulverbeugung und Synchrotron‐FTIR‐Mikrospektroskopie an ND3@MFM‐300(Al) bestätigen einen H‐D‐Austausch zwischen...
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