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Time of flight powder neutron diffraction has been used to study the structural changes on heating LiTi 2 O 4 from 25 to 1000 o C. A phase transition from the spinel to the ramsdellite form occurred between 875 and 925 o C; the two structure types coexisted, apparently in equilibrium over much of this range. About 300 o C below the transition, an anomalous change...
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