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In the ternary (Sr/Ca)‐Au‐Al phase space for 5–8 at % Sr/Ca and nearly equimolar mixture of Au and Al, five new NaZn13‐derivatives Sr/Ca(AuxAl1–x)12–13 were discovered and their atomic site preferences and electronic structures were studied: (1) at higher Au content, cubic SrAuxAl13–x [7.24(2) ≥ x ≥ 6.68(2)] shows no obvious atomic site preferences; (2) at lower Au content, tetragonal SrAuxAl13–x...
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