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Uniform Co–B nanoparticles were synthesized for the first time by chemical reduction of cobalt ion with borohydride in an oil-in-water microemulsion system comprising cyclohexane, polyethylene glycol, and water. The particle size was controlled by modulating the cyclohexane content. With the characterization of X-ray diffraction, selective area electronic diffraction, X-ray photoelectron spectroscopy,...
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