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This paper presents the results of a comprehensive investigation of single-phase calcium silicate hydrate (C S H) with known compositions using the combined capabilities of 29 Si magic angle spinning (MAS) NMR, powder X-ray diffraction (XRD), and chemical analysis of the solution and solid. C S H gels with C/S ratios ranging from 0.4 to 1.85 have been synthesized by hydration of highly...
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