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We report an ethanol‐mediated surfactant‐free solvothermal synthesis of phase‐pure Pnmm FeSb2 nanocrystals with an average size of 40 nm. The capping free growth of the nanocrystals resulted in the formation of inherent orthorhombic shapes. The nanocrystals were densified by spark plasma sintering to prepare a polycrystalline bulk material that consisted of 40–200 nm FeSb2 nanocrystal domains (nanocomposite)...
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