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Applying sealed vessel microwave heating at 180°C in toluene the arylation of aromatic and aliphatic aldehydes with arylboronic acids using 1–2mol% of Ni(acac) 2 as a catalyst can be performed efficiently within 10–30min providing the desired diarylmethanols or benzyl alcohols in good yields.
The palladium-catalyzed arylation of rac-(E)-3-acetoxy-1,3-diphenylprop-1-ene with arylboronic acids was studied under controlled microwave irradiation conditions. A variety of different catalysts, bases, and solvents were explored in order to achieve optimum yields in the shortest possible reaction times. The best isolated yields were obtained using Pd 2 (dba) 3 ·CHCl 3 /PPh...
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