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The dehydration of d-mannose and the demethanolization of methyl-α-d-mannopyranoside (MαMP) or methyl-α-d-mannofuranoside (MαMF) were examined using microwave-assisted heating for a 3-min irradiation at temperature from 120 to 280°C in ordinary or dry sulfolane without any catalyst. The microwave-assisted heating of MαMP and MαMF smoothly proceeded to selectively afford the anhydromannoses, 1,6-anhydro-β-d-mannopyranose...
An aqueous solution of glucose was reacted at temperatures from 200 to 400°C under atmospheric pressure using a continuous flow reactor. For reaction temperatures above 300°C, the liquid product yield was not sensitive to the temperature change; on the other hand, below 300°C, it decreased rapidly with decreasing temperature. 1,6-Anhydro-β-d-glucopyranose (AGP) and 1,6-anhydro-β-d-glucofuranose (AGF)...
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