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TiO2:Dy3+ powders without any secondary phases have been prepared by solid‐state reaction through the optimization of synthesis conditions, doping amount and subsequently through a purification step. The maximum dysprosium solubility was found at 0.43 mol% in the range 800–900°C. The Rietveld refinement was performed to calculate the amount of phases and lattice constants. The effect of synthesis...
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