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The synthesis of spinel-type lithium titanate, Li 4 Ti 5 O 12 , a promising anode material of secondary lithium-ion battery, from “inert” rutile TiO 2 , is investigated. On the purpose of increasing the reactivity of rutile TiO 2 , it is treated by concentrated HNO 3 . By applying such activated rutile TiO 2 as the titanium source in combination...
Spinel Li 4 Ti 5 O 12 was synthesized by a simple glycine-nitrate auto-combustion by applying aqueous medium and constricting the reactions in the pores of cellulose fibers. The products from the auto-combustion and further calcination at various temperatures were characterized by XRD, SEM, BET surface area and TEM examinations. Pure phase and well-crystallized nano-Li ...
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