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The mononuclear, tetrahedral iron and cobalt complexes, FeCl 2 (Hhpp) 2 , I, and CoCl 2 (Hhpp) 2 , II, are readily formed by the reaction of the metal (II) chloride with Hhpp. Compound II crystallized as blue blocks in the space group Fdd2. The reaction of I with LiMe yielded the trinuclear complex Fe 3 Cl 2 (hpp) 4 , III, which crystallized...
The reactions of Lihpp with vanadium(II) chloride, chromium(II) chloride and tetrakis(trifluoroacetato)dimolybdenum produce the dinuclear tetrabridged compounds V 2 (hpp) 4 , 1, Cr 2 (hpp) 4 , 2, and Mo 2 (hpp) 4 , 3. Compound 1 crystallizes as red blocks in the space group P1 with unit cell dimensions, a = 8.489(2), b = 9.709(2), c = 9.835(2) 9, α...
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