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One‐electron reductions of Mes*As=Fl* (1; Fl*=2,7‐di‐tert‐butylfluorenylidene, Mes*=2,4,6‐tBu3C6H2) and diarsaalkenes [1,2‐b]‐IF(=AsMes*)2 (2; IF=indenofluorene) with potassium led to the isolation of the arsenic‐centered radical anion salts 1K and 2K, respectively. The diradical dianion salts 2K2 and 3K2 were afforded by the reduction of 2 and 2,8‐tBu2‐[2,1‐b]‐IF(=AsMes*)2 (3) with an excess amount...
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