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We present an in-depth study of the UV-induced crosslinking of the polybutadiene domains in lamellar polystyrene-block-polybutadiene (PS-b-PB) block copolymer films. The crosslinking process is followed by a combination of depth-sensing indentation, Raman spectroscopy, and differential scanning calorimetry (DSC) investigations. Indentation assesses changes in the mechanical properties of the overall...
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