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In this study, a highly air stable and eco‐friendly methyl ammonium bismuth iodide (MA3Bi2I9) perovskite‐like material has been prepared. After physiochemical characterizations, the synthesized MA3Bi2I9 was utilized as photo‐catalyst towards hydrogen production. It is important to design and synthesize lead (Pb)‐free perovskite‐like material (MA3Bi2I9) for photo‐catalytic hydrogen‐production applications...