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A fluorous porous polymer stationary phase is photo‐patterned within a glass microfluidic chip to conduct CEC. During free radical‐initiated polymerization, extraneous polymer forms and contributes to excessive microfluidic channel clogging. Nitrobenzene is explored as free radical quencher to limit clogging by minimizing extraneous polymer formation and a number of initiator to quencher ratios are...
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