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The entrapment of silica-based microspheres, commonly used as stationary phases in chromatography, with an organic porous polymer based on poly(butyl acrylate-co-1,3-butanediol diacrylate) was explored. The spheres were immobilized by photopolymerization leading to entrapped beds within 75 μm i.d. fused silica capillaries, and were mechanically stable, resisting pressure drops of over 5600 psi (38...
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