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A new on-line method for the separation of vanadium (IV) and vanadium (V) as well as for the removal of ClO + mass spectral interference on vanadium determination by quadrupole-ICP-MS has been developed. The sample introduction system consists of a modified fused silica capillary coupled to a direct injection nebuliser (DIN), between the solvent delivery system and the ICP. Fused silica capillaries...
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