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The reactions between group 12 metals and the acidic TaF5 were studied in the anhydrous HF (aHF) solvent. We were able to prepare and characterize the first compounds containing metal M2+ cations and undecafluoridodimetallate anions – M(Ta2F11)2 (M=Cd, Hg) without the additional cations, anions or ligands included in the crystal structure. They both crystallize in P-1 space group with cell parameters...
Cd(AuF 6 ) 2 crystallizes at 200 K in the monoclinic space group C2/c (No. 15) with a=1116.7(7)pm, b=876.66(16)pm, c=1008.0(4)pm, β=118.026(5)° and Z=4. Cadmium atoms are in an octahedral environment of fluorine, and CdF 6 octahedra are sharing their vertices with six AuF 6 units on either side of the plane formed by the Cd atoms. On that way tridimensional network...
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