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Zirconium carbide (ZrC) was synthesized by solution‐based processing using versatile starting reagents including zirconium oxychloride octahydrate (ZrOCl2·8H2O, ZOC), acetylacetone (Hacac), and phenolic resin. Polyzirconoxane (PZO), obtained by chelation of Hacac to zirconium, was used to combine with phenolic resin to form a precursor for ZrC. It generated ZrC at a relatively low temperature (1550°C)...
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