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The microstructural characteristics of oxide films on 90Nb–10Zr (wt%) alloy in lithiated water were investigated to understand the oxidation process of β-Nb precipitates in Zr–1Nb (wt%) alloy. The outer layer of the alloy is faceted, and has loosely packed LiNbO3 particles. Pores and nano-sized LiNbO3 are present between the outer and the compact Nb2O5 inner layer. Nb2O5 reacted with LiOH to form...
The oxidation behavior of β-Nb precipitates in Zr–1Nb–0.2Bi alloy corroded in lithiated water with 0.01M LiOH at 360°C/18.6MPa was investigated by high-resolution transmission electron microscopy (HRTEM). From the HRTEM observation and the analysis for the oxide layer, the oxidation behavior of β-Nb precipitates corroded in lithiated water in early stage is as follows: β-Nb precipitates are first...
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