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Low‐cost, environment‐friendly aqueous Zn batteries have great potential for large‐scale energy storage, but the intercalation of zinc ions in the cathode materials is challenging and complex. Herein, the critical role of structural H2O on Zn2+ intercalation into bilayer V2O5·nH2O is demonstrated. The results suggest that the H2O‐solvated Zn2+ possesses largely reduced effective charge and thus reduced...
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