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The dissipation and residue status of a combination of fluopicolide and fosetyl‐aluminium (fosetyl‐Al) in citrus were evaluated in an experimental field. An efficient and sensitive liquid chromatography–tandem mass spectrometry, with rapid extraction, was carried out according to the SANTE guidelines. During the method validation, the recovery was within the range of 106.1–117.5, 94.4–115 and 85.4–109...