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The structural and thermoelectric properties of a series of icosahedral boron-rich solids, B 6 S 1−x obtained from the elements in a Ga melt were studied to estimate their potential as thermoelectric materials. Rietveld analysis of synchrotron and conventional X-ray powder data displayed the rhombohedral structure with the α-rhombohedral boron framework of B 12 icosahedra...
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