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The M-Cl (M=Fe, Co, Ni) boracites are prepared by a procedure consisting of solution mixing, evaporating to dryness, grinding and heating reaction in N 2 atmosphere. The lattice parameter and the phase transition temperatures of the boracites Co 3 B 7 O 13 Cl and Ni 3 B 7 O 13 Cl are investigated by means of X-ray diffraction, transmission...
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