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The reaction of Fe2(CO)9 and Bu 3t SnH yielded the bimetallic cluster complexes Fe2(μ-SnBu 2t )2(CO)8, 1, and Fe4(μ4-Sn)(μ-SnBu 2t )2(CO)16, 3. Compound 3 contains two Fe2(CO)8(μ-SnBu 2t ) groups held together by a central quadruply bridging tin atom, giving an overall bow-tie structure for the one tin and four iron atoms. Refluxing compound 1 in toluene solvent affords the complex Fe2[μ-SnBut...
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