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The synthesis of a SIPr [1,3‐bis(2,6‐diisopropylphenyl)‐imidazolin‐2‐ylidene] derived Kekulé diradicaloid with a tetrafluorophenylene spacer (3) has been described. Two synthetic routes have been reported to access 3. The cleavage of C−F bond of C6F6 by SIPr in the presence of BF3 led to double C−F activated compound with two tetrafluoro borate counter anions (2), which upon reduction by lithium metal...
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