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Triflic acid-functionalized Zr-TMS (zirconium oxide with a mesostructured framework; TMS, transition metal oxide mesoporous molecular sieves) catalysts have been synthesized by functionalizing triflic acid onto the walls of Zr-TMS via post synthesis method. The synthesized materials were characterized by powder XRD, N 2 -sorption, FT-IR spectroscopy, elemental analysis, solid-state 13...
Mesoporous Zr(OH) 4 was synthesized using N-cetyl-N,N,N-trimethyl ammonium bromide (CTMABr) as surfactant at atmospheric pressure and reflux conditions for 48h. After removal of the surfactant, the resulting mesoporous solid was functionalized with triflic acid (CF 3 SO 3 H, trifluoromethanesulfonic acid) in order to get the functionalized mesoporous ≡Zr O SO 2 CF...
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