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Oxygen evolution catalysed by calcium manganese and manganese‐only oxides was studied in 18O‐enriched water. Using membrane‐inlet mass spectrometry, we monitored the formation of the different O2 isotopologues 16O2, 16O18O and 18O2 in such reactions simultaneously with good time resolution. From the analysis of the data, we conclude that entirely different pathways of dioxygen formation catalysis...
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