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The reaction diffusion between Fe and Al during spark plasma sintering (SPS) was studied. Microstructural evolution was investigated by X-ray diffraction (XRD) and scanning electron microscopy (SEM) and the sintering kinetics was disclosed. The main interphase of the SPS sample was Fe2Al5 at 773–873 K. Ball-milling enabled a large number of lattice defects and grain boundaries thus the reaction kinetics...
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