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Two heterometallic photocatalysts were designed and probed for water reduction. Both [(bpy)2RuIINiII(L1)](ClO4)2 (1) and [(bpy)2RuIINiII(L2)2RuII(bpy)2](ClO4)2 (2) can generate the low‐valent precursor involved in hydride formation prior to dihydrogen generation. However, while the bimetallic [RuIINiII] (1) requires the presence of an external photosensitizer to trigger catalytic activity, the trimetallic...
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